Structures by: Halcrow M. A.

Total: 410

Bis[2,6-bis(5-methylpyrazol-3-yl)pyridine]iron(II) ditetrafluoroborate dihydrate

C26H26FeN10,2[BF4],2[H2O]

Roberts, Thomas D.Tuna, FlorianaMalkin, Tamsin L.Kilner, Colin A.Halcrow, Malcolm A.

Chemical Science (2012) 3, 2 349

a=13.7494(19)Å   b=13.7494(19)Å   c=35.336(3)Å

α=90.00°   β=90.00°   γ=90.00°

Bis[2,6-bis(5-methylpyrazol-3-yl)pyridine]iron(II) ditetrafluoroborate

C26H26FeN10,2[BF4]

Roberts, Thomas D.Tuna, FlorianaMalkin, Tamsin L.Kilner, Colin A.Halcrow, Malcolm A.

Chemical Science (2012) 3, 2 349

a=9.7481(2)Å   b=9.7481(2)Å   c=17.6848(5)Å

α=90.00°   β=90.00°   γ=90.00°

Bis[2,6-bis(5-methylpyrazol-3-yl)pyridine]iron(II) ditetrafluoroborate

C26H26FeN10,2[BF4]

Roberts, Thomas D.Tuna, FlorianaMalkin, Tamsin L.Kilner, Colin A.Halcrow, Malcolm A.

Chemical Science (2012) 3, 2 349

a=9.8046(5)Å   b=9.8046(5)Å   c=17.8869(13)Å

α=90.00°   β=90.00°   γ=90.00°

2,6-bis(5-methylpyrazol-3-yl)pyridine methanol solvate

C13H13N5,CH4O

Roberts, Thomas D.Tuna, FlorianaMalkin, Tamsin L.Kilner, Colin A.Halcrow, Malcolm A.

Chemical Science (2012) 3, 2 349

a=10.0640(4)Å   b=11.6546(5)Å   c=12.3944(6)Å

α=90.00°   β=90.00°   γ=90.00°

C22H18B2F8FeN10

C22H18B2F8FeN10

Money, Victoria A.Evans, Ivana RadosavljevicHalcrow, Malcolm A.Goeta, Andrés EHoward, Judith A. K.

Chemical communications (Cambridge, England) (2003) 1 158-159

a=8.4615(17)Å   b=8.3695(17)Å   c=18.759(4)Å

α=90.00°   β=97.15(3)°   γ=90.00°

C22H18B2F8FeN10

C22H18B2F8FeN10

Money, Victoria A.Evans, Ivana RadosavljevicHalcrow, Malcolm A.Goeta, Andrés EHoward, Judith A. K.

Chemical communications (Cambridge, England) (2003) 1 158-159

a=8.4098(4)Å   b=8.4731(4)Å   c=18.2909(9)Å

α=90.00°   β=98.5750(10)°   γ=90.00°

Bis(2,6-bis(hydrazonomethyl)pyridine)copper(ii) diperchlorate bis-acetone solvate

C14H18CuN10,2[ClO4],2[C3H6O]

Halcrow, Malcolm A.Kilner, Colin A.Wolowska, JoannaMcInnes, Eric J. L.Bridgeman, Adam J.

New Journal of Chemistry (2004) 28, 2 228

a=21.8166(4)Å   b=7.3939(1)Å   c=21.5138(3)Å

α=90.00°   β=118.0158(7)°   γ=90.00°

Bis(2,6-bis(oximomethyl)pyridine)copper(ii) diperchlorate bis- acetone solvate

C14H14CuN6O4,2[ClO4],2[C3H6O]

Halcrow, Malcolm A.Kilner, Colin A.Wolowska, JoannaMcInnes, Eric J. L.Bridgeman, Adam J.

New Journal of Chemistry (2004) 28, 2 228

a=7.1602(1)Å   b=13.2144(3)Å   c=17.3567(3)Å

α=107.6773(12)°   β=95.9665(13)°   γ=103.6906(8)°

Bis(2,6-bis(oximomethyl)pyridine)copper(ii) diperchlorate bis- acetone solvate

C14H14CuN6O4,2[ClO4],2[C3H6O]

Halcrow, Malcolm A.Kilner, Colin A.Wolowska, JoannaMcInnes, Eric J. L.Bridgeman, Adam J.

New Journal of Chemistry (2004) 28, 2 228

a=6.9012(2)Å   b=13.1087(3)Å   c=17.5759(4)Å

α=107.2644(16)°   β=94.6164(16)°   γ=105.2984(10)°

Bis(2,6-bis(oximomethyl)pyridine)copper(ii) diperchlorate bis- acetone solvate

C14H14CuN6O4,2[ClO4],2[C3H6O]

Halcrow, Malcolm A.Kilner, Colin A.Wolowska, JoannaMcInnes, Eric J. L.Bridgeman, Adam J.

New Journal of Chemistry (2004) 28, 2 228

a=6.8580(2)Å   b=13.0630(3)Å   c=17.5689(5)Å

α=107.2649(14)°   β=94.1119(11)°   γ=105.6603(10)°

Chloro-tris[5-tertbutylpyrazole]zinc(II) bis[nido-undecahydro-7,8-dicarbanonaborato]cobalt(III)

C21H36ClN6Zn,C4H22B18Co

Renard, Sylvie L.Franken, AndreasKilner, Colin A.Kennedy, John D.Halcrow, Malcolm A.

New Journal of Chemistry (2002) 26, 11 1634

a=15.0060(1)Å   b=17.6110(2)Å   c=17.9379(2)Å

α=84.1973(3)°   β=65.6599(4)°   γ=82.3658(5)°

[Chloro-tris(5-tertbutylpyrazole)zinc(II)] [6,7,8,9,10-pentabromo-pentahydro-closo-1-carbanonaborate] hydrate

C21H36ClN6Zn,CH5B9Br5,OH2

Renard, Sylvie L.Franken, AndreasKilner, Colin A.Kennedy, John D.Halcrow, Malcolm A.

New Journal of Chemistry (2002) 26, 11 1634

a=24.0110(2)Å   b=12.3005(1)Å   c=27.2856(3)Å

α=90.00°   β=90.00°   γ=90.00°

[Chloro-tris(5-tertbutylpyrazole)zinc(II)][1-phenyl-nonahydro-closo-1- carbanonaborate] pentane solvate

C21H36ClN6Zn,C7H14B9,0.2[C5H12]

Renard, Sylvie L.Franken, AndreasKilner, Colin A.Kennedy, John D.Halcrow, Malcolm A.

New Journal of Chemistry (2002) 26, 11 1634

a=10.8007(1)Å   b=15.4087(1)Å   c=24.7967(3)Å

α=100.3662(4)°   β=97.0776(4)°   γ=100.9195(6)°

Catena-[tris(5-tertbutylpyrazole)sulfatocobalt(II)]

C21H36CoN6O4S

Jones, Leigh F.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2007) 31, 8 1530

a=10.7470(2)Å   b=13.1706(2)Å   c=18.1220(4)Å

α=90.00°   β=90.00°   γ=90.00°

Dichloro-bis-(5-phenylpyrazole)zinc chloroform solvate

C18H16Cl2N4Zn,2[CHCl3]

Day, JonathanMarriott, Katie E. R.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2010) 34, 1 52

a=8.8197(11)Å   b=12.0309(13)Å   c=12.1267(15)Å

α=98.231(6)°   β=104.297(6)°   γ=104.816(6)°

Bis(5-cyclohexylpyrazole)dichlorozinc(ii)

C18H28Cl2N4Zn

Day, JonathanMarriott, Katie E. R.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2010) 34, 1 52

a=10.6333(9)Å   b=11.5074(11)Å   c=17.8610(17)Å

α=90.00°   β=97.665(5)°   γ=90.00°

Chloro-tris(5-phenylpyrazole)zinc(II) chloride

C27H24ClN6Zn,Cl

Day, JonathanMarriott, Katie E. R.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2010) 34, 1 52

a=17.685(2)Å   b=17.185(2)Å   c=17.758(3)Å

α=90.00°   β=90.00°   γ=90.00°

Chloro-tris(5-cyclohexylpyrazole)zinc(II) nitrate

C27H42ClN6Zn,NO3

Day, JonathanMarriott, Katie E. R.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2010) 34, 1 52

a=11.9059(9)Å   b=12.3024(9)Å   c=12.4108(9)Å

α=66.546(3)°   β=74.875(4)°   γ=71.417(4)°

Bromo-tris(5-cyclohexylpyrazole)zinc(II) nitrate hydrate

C27H42BrN6Zn,NO3,H2O

Day, JonathanMarriott, Katie E. R.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2010) 34, 1 52

a=11.5875(16)Å   b=15.191(3)Å   c=18.270(3)Å

α=90.00°   β=90.00°   γ=90.00°

Chloro-tris(5-cyclohexylpyrazole)zinc(II) perchlorate

C27H42ClN6Zn,ClO4

Day, JonathanMarriott, Katie E. R.Kilner, Colin A.Halcrow, Malcolm A.

New Journal of Chemistry (2010) 34, 1 52

a=24.414(3)Å   b=16.933(2)Å   c=19.071(4)Å

α=90.00°   β=126.019(5)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)-4-(thiomorpholin-1-yl)pyridine]iron(II) di-tetrafluoroborate monohydrate

C30H32FeN12S2,2[BF4],H2O

Laurynas PukenasFlorence BennEdmund LovellAmedeo SantoroLaurence J. Kershaw CookMalcolm A. HalcrowStephen D. Evans

Journal of Materials Chemistry C (2015) 3, 7890-7896

a=11.4182(5)Å   b=13.3351(7)Å   c=13.8880(8)Å

α=85.289(4)°   β=68.183(4)°   γ=66.115(4)°

Bis[2,6-di(pyrazol-1-yl)-4-(thiomorpholin-1-yl)pyridine]iron(II) diperchlorate hydrate (1/0.33)

C30H32FeN12S2,2[ClO4],0.33[H2O]

Laurynas PukenasFlorence BennEdmund LovellAmedeo SantoroLaurence J. Kershaw CookMalcolm A. HalcrowStephen D. Evans

Journal of Materials Chemistry C (2015) 3, 7890-7896

a=11.5334(6)Å   b=13.2237(7)Å   c=14.0842(8)Å

α=85.594(4)°   β=68.230(5)°   γ=65.418(5)°

Bis[2,6-di(pyrazol-1-yl)-4-(thiomorpholin-1-yl)pyridine]iron(II) bis-trifluoromethanesulfonate

C30H32FeN12S2,2[CF3O3S]

Laurynas PukenasFlorence BennEdmund LovellAmedeo SantoroLaurence J. Kershaw CookMalcolm A. HalcrowStephen D. Evans

Journal of Materials Chemistry C (2015) 3, 7890-7896

a=12.4186(7)Å   b=13.3433(7)Å   c=14.2652(6)Å

α=75.472(4)°   β=67.419(5)°   γ=64.190(5)°

C52B6CoF3N7O2

C52B6CoF3N7O2

Norbani AbdullahNur Linahafizza Md NoorAbdul Rahman NordinMalcolm A. HalcrowDouglas R. MacFarlaneManoj A. LazarJennifer M. PringleDuncan W. BruceBertrand DonnioBenoit Heinrich

Journal of Materials Chemistry C (2015) 3, 2491-2499

a=17.1066(13)Å   b=9.3515(7)Å   c=21.8195(16)Å

α=90°   β=107.6370(10)°   γ=90°

2-(Pyrazol-1-yl)-6-(1,2,4-triazol-1-yl)pyridine

C10H8N6

Galadzhun, IuriiCapel Berdiell, IzarShahid, NamrahHalcrow, Malcolm A.

CrystEngComm (2019) 21, 42 6330

a=12.5794(9)Å   b=3.8549(3)Å   c=20.4981(14)Å

α=90.00°   β=103.627(7)°   γ=90.00°

2-Fluoro-6-(pyrazol-1-yl)pyridine

C8H6FN3

Galadzhun, IuriiCapel Berdiell, IzarShahid, NamrahHalcrow, Malcolm A.

CrystEngComm (2019) 21, 42 6330

a=4.0393(1)Å   b=11.2187(4)Å   c=16.2922(4)Å

α=90.00°   β=90.00°   γ=90.00°

Hexafluorotetrakis(3{5}-tertbutylpyrazolido)octakis(5-tertbutylpyrazole)- hexacopper(II) difluoride bischloroform hemi-heptane solvate

C84H140Cu6F6N24,2F,2[CHCl3],0.5[C7H16]

Liu, XiaomingMcLaughlin, Abbie C.de Miranda, Marcelo P.McInnes, Eric J. L.Kilner, Colin A.Halcrow, Malcolm A.

Chemical Communications (2002) 24 2978

a=12.9428(1)Å   b=20.4550(1)Å   c=24.9037(2)Å

α=67.7688(4)°   β=82.1704(4)°   γ=74.9426(3)°

Bis(disulfide)-cryptophane-0.0

C48H44O8S4,C3H6NO,C4H10O,

Little, Marc A.Halcrow, Malcolm A.Hardie, Michaele J.

Chemical communications (Cambridge, England) (2013) 49, 15 1512-1514

a=11.768(7)Å   b=15.158(8)Å   c=15.531(8)Å

α=90.075(5)°   β=104.370(5)°   γ=103.986(11)°

Tris[pyrazol-3-ylpyrazine]iron(II) ditetrafluoroborate trihydrate

C21H18FeN12,2[BF4],3[H2O]

Jonathan J. LoughreyTim P. ComynDavid C. ApperleyMarc A. LittleMalcolm A. Halcrow

Chem.Commun. (2014) 50, 7601

a=12.6729(5)Å   b=12.6729(5)Å   c=10.9338(6)Å

α=90.00°   β=90.00°   γ=120.00°

Tris[pyrazol-3-ylpyrazine]iron(II) ditetrafluoroborate trihydrate

C21H18FeN12,2[BF4],3[H2O]

Jonathan J. LoughreyTim P. ComynDavid C. ApperleyMarc A. LittleMalcolm A. Halcrow

Chem.Commun. (2014) 50, 7601

a=12.6653(9)Å   b=12.6653(9)Å   c=11.0258(12)Å

α=90.00°   β=90.00°   γ=120.00°

Tris[pyrazol-3-ylpyrazine]iron(II) ditetrafluoroborate trihydrate

C21H18FeN12,2[BF4],3[H2O]

Jonathan J. LoughreyTim P. ComynDavid C. ApperleyMarc A. LittleMalcolm A. Halcrow

Chem.Commun. (2014) 50, 7601

a=12.6778(7)Å   b=12.6778(7)Å   c=10.9308(8)Å

α=90.00°   β=90.00°   γ=120.00°

Tris[pyrazol-3-ylpyrazine]iron(II) ditetrafluoroborate trihydrate

C21H18FeN12,2[BF4],3[H2O]

Jonathan J. LoughreyTim P. ComynDavid C. ApperleyMarc A. LittleMalcolm A. Halcrow

Chem.Commun. (2014) 50, 7601

a=12.660(2)Å   b=12.660(2)Å   c=10.9359(15)Å

α=90.00°   β=90.00°   γ=120.00°

Bis-[2,6-dipyrazol-1-ylpyridine]iron(II) ditetrafluoroborate

[C22H18FeN10]2[BF4]

Holland, Joanne M.Kilner, Colin A.Thornton-Pett, MarkHalcrow, Malcolm A.McAllister, Judith A.Lu, Zhibao

Chemical Communications (2001) 6 577

a=8.5301(3)Å   b=8.5518(4)Å   c=19.1757(5)Å

α=90.00°   β=94.9043(24)°   γ=90.00°

Bis-[2,6-dipyrazol-1-ylpyridine]iron(II) ditetrafluoroborate

[C22H18FeN10]2[BF4]

Holland, Joanne M.Kilner, Colin A.Thornton-Pett, MarkHalcrow, Malcolm A.McAllister, Judith A.Lu, Zhibao

Chemical Communications (2001) 6 577

a=8.4947(2)Å   b=8.5070(2)Å   c=19.0535(6)Å

α=90.00°   β=95.7050(18)°   γ=90.00°

Bis-[2,6-dipyrazol-1-ylpyridine]iron(II) ditetrafluoroborate

[C22H18FeN10]2[BF4]

Holland, Joanne M.Kilner, Colin A.Thornton-Pett, MarkHalcrow, Malcolm A.McAllister, Judith A.Lu, Zhibao

Chemical Communications (2001) 6 577

a=8.4977(3)Å   b=8.5665(3)Å   c=18.4299(8)Å

α=90.00°   β=98.0931(12)°   γ=90.00°

Bis-[2,6-dipyrazol-1-ylpyridine]iron(II) ditetrafluoroborate

[C22H18FeN10]2[BF4]

Holland, Joanne M.Kilner, Colin A.Thornton-Pett, MarkHalcrow, Malcolm A.McAllister, Judith A.Lu, Zhibao

Chemical Communications (2001) 6 577

a=8.4575(2)Å   b=8.5233(2)Å   c=18.3756(4)Å

α=90.00°   β=98.2896(13)°   γ=90.00°

C22H18CuN10,2(BF4)

C22H18CuN10,2(BF4)

Leech, Michael A.Howard, Judith A. K.Dahaoui, SlimaneSolanki, Nayan K.Halcrow, Malcolm A.

Chemical Communications (1999) 22 2245

a=8.4141(9)Å   b=8.4747(9)Å   c=18.6833(19)Å

α=90.00°   β=97.371(2)°   γ=90.00°

C22H18CuN10,2(BF4)

C22H18CuN10,2(BF4)

Leech, Michael A.Howard, Judith A. K.Dahaoui, SlimaneSolanki, Nayan K.Halcrow, Malcolm A.

Chemical Communications (1999) 22 2245

a=8.4047(6)Å   b=25.3897(18)Å   c=18.6676(13)Å

α=90.00°   β=97.2050(10)°   γ=90.00°

Bis[(2,6-di(pyrazol-1-yl)pyridine]ruthenium(II) ditetrafluoroborate

C22H18N10Ru,2[BF4]

Halcrow, Malcolm A.

Chemical Communications (2010) 46, 26 4761-4763

a=8.5703(8)Å   b=8.6188(7)Å   c=18.6937(16)Å

α=90.00°   β=97.706(6)°   γ=90.00°

Iodo-tris[5-tertbutylpyrazole]zinc(II) iodide dichloromethane solvate

C21H36IN6Zn,I,CH2Cl2

Liu, XiaomingKilner, Colin A.Halcrow, Malcolm A.

Chemical Communications (2002) 7 704

a=10.4896(1)Å   b=19.2431(2)Å   c=30.6552(4)Å

α=90.00°   β=90.00°   γ=90.00°

Chloro-tris[5-tertbutylpyrazole]zinc(II) chloride hemipentane solvate

C21H36ClN6Zn,Cl,0.5[C5H12]

Liu, XiaomingKilner, Colin A.Halcrow, Malcolm A.

Chemical Communications (2002) 7 704

a=17.1001(3)Å   b=10.7850(2)Å   c=17.9314(3)Å

α=90.00°   β=115.1510(7)°   γ=90.00°

Bromo-tris[5-tertbutylpyrazole]zinc(II) bromide hemipentane solvate

C21H36BrN6Zn,Br,0.5[C5H12]

Liu, XiaomingKilner, Colin A.Halcrow, Malcolm A.

Chemical Communications (2002) 7 704

a=17.3353(2)Å   b=10.5568(2)Å   c=18.4428(2)Å

α=90.00°   β=114.9379(9)°   γ=90.00°

Bis(2,6-di(pyrazol-1-yl)pyridine)iron(ii) ditetrafluoroborate

C22H18FeN10,2[BF4]

Tovee, Clare A.Kilner, Colin A.Thomas, James A.Halcrow, Malcolm A.

CrystEngComm (2009) 11, 10 2069

a=8.5257(17)Å   b=8.5083(16)Å   c=19.230(4)Å

α=90.00°   β=95.224(9)°   γ=90.00°

Bis(2,2':6',2''-terpyridine)ruthenium(ii) ditetrafluoroborate

C30H22N6Ru,2[BF4]

Tovee, Clare A.Kilner, Colin A.Thomas, James A.Halcrow, Malcolm A.

CrystEngComm (2009) 11, 10 2069

a=12.716(4)Å   b=12.440(5)Å   c=19.237(7)Å

α=90.00°   β=98.135(17)°   γ=90.00°

Dichloro-bis[5-amino-3-(pyrid-2-yl)pyrazole]manganese(II) dimethanol solvate (1.2CH~3~OH)

C16H16Cl2MnN8,2[CH4O]

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=18.9615(3)Å   b=11.9420(3)Å   c=12.8415(2)Å

α=90.00°   β=125.6748(10)°   γ=90.00°

Dichloro-bis[5-amino-3-(pyrid-2-yl)pyrazole]iron(III) chloride tetrakis-methanol solvate (2.4CH~3~OH)

C16H16Cl2FeN8,Cl,4[CH4O]

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=10.7275(2)Å   b=11.6620(2)Å   c=11.9305(2)Å

α=95.9291(6)°   β=96.0695(6)°   γ=110.0749(10)°

Bis[5-amino-3-(pyrid-2-yl)pyrazole][acetonitrile]copper(II) diperchlorate (4)

C18H19CuN9,2[ClO4]

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=20.5384(7)Å   b=8.2388(2)Å   c=14.5781(6)Å

α=90.00°   β=101.4093(13)°   γ=90.00°

Bis[5-amino-3-(pyrid-2-yl)pyrazole]copper(II) diperchlorate methanol solvate (3.CH~3~OH)

C16H16CuN8,2[ClO4],CH4O

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=7.2901(3)Å   b=28.8637(8)Å   c=11.8758(6)Å

α=90.00°   β=107.874(2)°   γ=90.00°

Nitrato-bis(5-amino-3-(pyrid-2-yl)pyrazole)copper(ii) nitrate hydrate (0.5/0.13) (5.xH!2$O; x = 0.13)

C16H16CuN9O3,NO3,0.13[H2O]

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=14.3848(2)Å   b=16.2140(2)Å   c=34.3029(5)Å

α=90.00°   β=90.00°   γ=90.00°

Nitrato-bis[5-amino-3-(pyrid-2-yl)pyrazole]zinc(II) nitrate hydrate (0.5/0.29) (5.xH~2~O; x = 0.29)

C16H16N9O3Zn,NO3,0.29[H2O]

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=14.1680(1)Å   b=16.4064(2)Å   c=35.0658(4)Å

α=90.00°   β=90.00°   γ=90.00°

Tetrakis(5-amino-3-{pyrid-2-yl}pyrazolido)dicopper(II) hydrate (0.5/0.25) (7.xH~2~O; x = 0.25)

C32H28Cu2N16,0.25[H2O]

Jones, Leigh F.Camm, Kenneth D.Kilner, Colin A.Halcrow, Malcolm A.

CrystEngComm (2006) 8, 9 719

a=12.3753(7)Å   b=17.1300(13)Å   c=16.3243(12)Å

α=90.00°   β=110.892(4)°   γ=90.00°

Bis(2,6-bis(3-(hydroxymethyl)pyrazol-1-yl)pyridine)iron(ii) diperchlorate, alpha polymorph

C26H26FeN10O4,2[ClO4]

Jérôme ElhaïkColin A. KilnerMalcolm A. Halcrow

CrystEngComm (2005) 7, 23 151

a=16.2700(6)Å   b=11.3714(4)Å   c=16.6040(6)Å

α=90.00°   β=91.6986(16)°   γ=90.00°

Bis(2,6-bis(3-(hydroxymethyl)pyrazol-1-yl)pyridine)iron(ii) diperchlorate, beta polymorph

C26H26FeN10O4,2[ClO4]

Jérôme ElhaïkColin A. KilnerMalcolm A. Halcrow

CrystEngComm (2005) 7, 23 151

a=20.1578(2)Å   b=10.0249(1)Å   c=16.2228(1)Å

α=90.00°   β=108.3160(8)°   γ=90.00°

Bis(2,6-bis(3-hydroxymethylpyrazol-1-yl)pyridine)iron(ii) diperchlorate acetonitrile solvate

C26H26FeN10O4,2[ClO4],0.75[C2H3N]

Jérôme ElhaïkColin A. KilnerMalcolm A. Halcrow

CrystEngComm (2005) 7, 23 151

a=22.8535(2)Å   b=11.6789(1)Å   c=27.9986(3)Å

α=90.00°   β=107.6122(5)°   γ=90.00°

Bis(2,6-bis(3-hydroxymethylpyrazol-1-yl)pyridine)iron(ii) diperchlorate acetonitrile solvate

C26H26FeN10O4,2[ClO4],0.75[C2H3N]

Jérôme ElhaïkColin A. KilnerMalcolm A. Halcrow

CrystEngComm (2005) 7, 23 151

a=22.4565(2)Å   b=11.6040(1)Å   c=27.9163(3)Å

α=90.00°   β=107.3812(4)°   γ=90.00°

2-(4-Pyridyl)malondialdehyde Sesquihydrate

C8H7NO2,1.5[H2O]

Tovee, Clare A.Kilner, Colin A.Thomas, Jim A.Halcrow, Malcolm A.

CrystEngComm (2007) 9, 5 361

a=24.2053(5)Å   b=3.7445(1)Å   c=20.9542(7)Å

α=90.00°   β=121.3149(11)°   γ=90.00°

(1,8-Bis(5-methylsalicylaldiminato)-3,6-diazaoctane)iron(iii) hexafluorophosphate

C22H28FeN4O2,F6P

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=10.3752(9)Å   b=13.3931(11)Å   c=19.3373(17)Å

α=107.903(4)°   β=90.780(4)°   γ=101.238(4)°

(1,8-Bis(2-hydroxy-1-naphthaldiminato)-3,6- diazaoctane)iron(iii) hexafluorophosphate diethylether solvate

C28H28FeN4O2,PF6,C4H10O

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=14.1874(12)Å   b=15.7976(13)Å   c=29.091(3)Å

α=90.00°   β=90.00°   γ=90.00°

(1,8-Bis(5-tert-butylsalicylaldiminato)-3,6- diazaoctane)iron(iii) nitrate 1,2-dichloroethane solvate

C28H40FeN4O2,NO3,C2H4Cl2

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=16.1177(7)Å   b=21.6263(10)Å   c=9.8296(7)Å

α=90.00°   β=90.7226(19)°   γ=90.00°

(1,8-Bis(salicylaldiminato)-3,6-diazaoctane)iron(iii) hexafluorophosphate

C20H24FeN4O2,F6P

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=9.6187(12)Å   b=27.768(3)Å   c=18.009(2)Å

α=90.00°   β=93.033(8)°   γ=90.00°

(1,8-Bis(salicylaldiminato)-3,6-diazaoctane)iron(iii) hexafluorophosphate

C20H24FeN4O2,F6P

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=9.5581(8)Å   b=27.316(2)Å   c=17.9457(15)Å

α=90.00°   β=92.340(5)°   γ=90.00°

Bis(3-(pyrid-2-yl)-5-aminopyrazole)bromocopper(ii) bromide methanol solvate

C16H16BrCuN8,Br,CH4O

Pask, Christopher M.Camm, Kenneth D.Bullen, Neil J.Carr, Michael J.Clegg, WilliamKilner, Colin A.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2006) 5 662-664

a=8.8159(18)Å   b=21.777(5)Å   c=22.260(5)Å

α=90.00°   β=90.00°   γ=90.00°

Bis(5-amino-3-(pyrid-2-yl)pyrazole)aquacopper(ii) sulfate monohydrate mono-methanol solvate

C16H18CuN8O,SO4,CH4O,H2O

Pask, Christopher M.Camm, Kenneth D.Bullen, Neil J.Carr, Michael J.Clegg, WilliamKilner, Colin A.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2006) 5 662-664

a=10.1984(11)Å   b=12.8621(14)Å   c=17.3027(19)Å

α=90.00°   β=102.705(1)°   γ=90.00°

Bis(2-[2-{2',5'-dihydroxybenzaldimino}ethyl]pyridine)dicopper(II) ditetrafluoroborate nitromethane solvate

[C28H26N4O4Cu2][BF4]2CH3NO2

Li, PeiyiSolanki, Nayan K.Ehrenberg, HelmutFeeder, NeilDavies, John E.Rawson, Jeremy M.Halcrow, Malcolm A.

Journal of the Chemical Society, Dalton Transactions (2000) 10 1559

a=14.605(4)Å   b=12.551(3)Å   c=11.021(3)Å

α=106.74(2)°   β=75.19(3)°   γ=71.34(2)°

[N-(2-{pyrid-2-ylmethylamino}ethyl)-2,5-dihydroxybenzaldimino]copper(II) perchlorate

[C15H16N3O2Cu]ClO4

Li, PeiyiSolanki, Nayan K.Ehrenberg, HelmutFeeder, NeilDavies, John E.Rawson, Jeremy M.Halcrow, Malcolm A.

Journal of the Chemical Society, Dalton Transactions (2000) 10 1559

a=7.683(1)Å   b=11.404(1)Å   c=19.242(1)Å

α=90.000°   β=99.56(1)°   γ=90.000°

2,6-bis(4-chloropyrazol-1-yl)pyridine

C11H7Cl2N5

Pritchard, RuthLazar, HananeBarrett, Simon A.Kilner, Colin A.Asthana, SaketCarbonera, ChiaraLétard, Jean-FrançoisHalcrow, Malcolm A.

Dalton Transactions (2009) 33 6656-6666

a=16.329(3)Å   b=3.8130(7)Å   c=20.215(3)Å

α=90.00°   β=104.231(9)°   γ=90.00°

2,6-bis(4-bromopyrazol-1-yl)pyridine

C11H7Br2N5

Pritchard, RuthLazar, HananeBarrett, Simon A.Kilner, Colin A.Asthana, SaketCarbonera, ChiaraLétard, Jean-FrançoisHalcrow, Malcolm A.

Dalton Transactions (2009) 33 6656-6666

a=16.1867(15)Å   b=3.8789(3)Å   c=20.1485(17)Å

α=90.00°   β=103.757(3)°   γ=90.00°

Bis[2,6-di(4-chloropyrazol-1-yl)pyridine]iron(II) ditetrafluoroborate

C22H14Cl4FeN10,2[BF4]

Pritchard, RuthLazar, HananeBarrett, Simon A.Kilner, Colin A.Asthana, SaketCarbonera, ChiaraLétard, Jean-FrançoisHalcrow, Malcolm A.

Dalton Transactions (2009) 33 6656-6666

a=17.1919(12)Å   b=41.318(3)Å   c=13.4331(10)Å

α=90.00°   β=90.00°   γ=90.00°

Bis[2,6-bis{4-iodopyrazol-1-yl}pyridine]iron(II) ditetrafluoroborate bis-acetone solvate

C22H14FeI4N10,2[BF4],2[C3H6O]

Pritchard, RuthLazar, HananeBarrett, Simon A.Kilner, Colin A.Asthana, SaketCarbonera, ChiaraLétard, Jean-FrançoisHalcrow, Malcolm A.

Dalton Transactions (2009) 33 6656-6666

a=11.4909(1)Å   b=10.0039(1)Å   c=35.3093(4)Å

α=90.00°   β=90.6172(4)°   γ=90.00°

Bis(2,6-bis(4-iodopyrazol-1-yl)pyridine)iron(ii) ditetrafluoroborate mono-acetone solvate

C22H14FeI4N10,2[BF4],C3H6O

Pritchard, RuthLazar, HananeBarrett, Simon A.Kilner, Colin A.Asthana, SaketCarbonera, ChiaraLétard, Jean-FrançoisHalcrow, Malcolm A.

Dalton Transactions (2009) 33 6656-6666

a=15.6789(2)Å   b=16.5181(2)Å   c=15.9708(2)Å

α=90.00°   β=96.3400(10)°   γ=90.00°

(1,8-Bis(salicylaldiminato)-3,6-diazaoctane)iron(iii) tetraphenylborate hemi-(1,2-dichloroethane) solvate

C20H24FeN4O2,C24H20B,0.5[C2H4Cl2]

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=26.180(5)Å   b=10.750(2)Å   c=28.620(6)Å

α=90.00°   β=102.09(3)°   γ=90.00°

(1,8-Bis(salicylaldiminato)-3,6-diazaoctane)iron(iii) perchlorate

C20H24FeN4O2,ClO4

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=17.8864(15)Å   b=13.7970(11)Å   c=27.951(3)Å

α=90.00°   β=100.881(5)°   γ=90.00°

(1,8-Bis(salicylaldiminato)-3,6-diazaoctane)iron(iii) tetraphenylborate hemi-acetone solvate

C20H24FeN4O2,C24H20B,0.5[C3H6O]

Pritchard, RuthBarrett, Simon A.Kilner, Colin A.Halcrow, Malcolm A.

Dalton Transactions (2008) 24 3159-3168

a=25.977(2)Å   b=10.8833(12)Å   c=28.562(3)Å

α=90.00°   β=103.321(5)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) ditetrafluoroborate

C22H18FeN10,2[BF4]

Carbonera, ChiaraKilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 13 1284-1292

a=8.5468(8)Å   b=8.5592(7)Å   c=19.1536(18)Å

α=90.00°   β=95.640(5)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) 1.56:0.44 tetrafluoroborate: perchlorate salt

C22H18FeN10,1.56[BF4],0.44[ClO4]

Carbonera, ChiaraKilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 13 1284-1292

a=8.5441(6)Å   b=8.5611(6)Å   c=19.2084(13)Å

α=90.00°   β=95.582(4)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) 1.56:0.44 tetrafluoroborate: perchlorate salt

C22H18FeN10,1.56[BF4],0.44[ClO4]

Carbonera, ChiaraKilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 13 1284-1292

a=8.5049(3)Å   b=8.5662(4)Å   c=18.4963(7)Å

α=90.00°   β=98.411(2)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) 0.87:1.13 tetrafluoroborate: perchlorate salt

C22H18FeN10,0.87[BF4],1.13[ClO4]

Carbonera, ChiaraKilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 13 1284-1292

a=8.5693(3)Å   b=8.5868(3)Å   c=19.3352(7)Å

α=90.00°   β=95.597(2)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) 0.32:1.68 tetrafluoroborate: perchlorate salt

C22H18FeN10,0.32[BF4],1.68[ClO4]

Carbonera, ChiaraKilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 13 1284-1292

a=14.4602(17)Å   b=9.3419(11)Å   c=20.202(2)Å

α=90.00°   β=99.320(6)°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) 0.87:1.13 tetrafluoroborate: perchlorate salt

C22H18FeN10,0.87[BF4],1.13[ClO4]

Carbonera, ChiaraKilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 13 1284-1292

a=8.5348(3)Å   b=8.5892(3)Å   c=18.6089(6)Å

α=90.00°   β=98.567(2)°   γ=90.00°

Bis(5-(4-fluorophenyl)pyrazolido)-bis(5-(4- fluorophenyl)pyrazole)copper(ii)

C36H26CuF4N8

Mokuolu, Q. FolshadeFoguet-Albiol, DolosJones, Leigh F.Wolowska, JoannaKowalczyk, Radoslaw M.Kilner, Colin A.Christou, GeorgeMcGowan, Patrick C.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 14 1392-1399

a=36.1535(6)Å   b=7.69370(10)Å   c=10.9951(2)Å

α=90.00°   β=90.00°   γ=90.00°

Tetrakis(3(5)-(pyrid-2-yl)pyrazolido)dicopper(ii) dichloroform hemihydrate solvate

C32H24Cu2N12,2[CHCl3],0.5[H2O]

Mokuolu, Q. FolshadeFoguet-Albiol, DolosJones, Leigh F.Wolowska, JoannaKowalczyk, Radoslaw M.Kilner, Colin A.Christou, GeorgeMcGowan, Patrick C.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 14 1392-1399

a=27.6069(3)Å   b=17.8695(2)Å   c=32.0957(4)Å

α=90.00°   β=90.00°   γ=90.00°

Octakis(3(5)-phenylpyrazolido)tetracopper(ii) hemi-pentane solvate

C72H56Cu4N16,0.5[C5H12]

Mokuolu, Q. FolshadeFoguet-Albiol, DolosJones, Leigh F.Wolowska, JoannaKowalczyk, Radoslaw M.Kilner, Colin A.Christou, GeorgeMcGowan, Patrick C.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 14 1392-1399

a=18.978(4)Å   b=17.233(3)Å   c=22.798(5)Å

α=90.00°   β=114.117(8)°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) ditetrafluoroborate monohydrate

C18H24FeN10,2[BF4],H2O

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=9.3582(1)Å   b=22.4857(3)Å   c=12.6267(2)Å

α=90.00°   β=101.5842(5)°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) dinitrate mono-nitromethane solvate

C18H24FeN10,2[NO3],CH3NO2

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=11.6918(12)Å   b=12.9226(14)Å   c=17.923(2)Å

α=90.00°   β=90.00°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) dinitrate mono-nitromethane solvate

C18H24FeN10,2[NO3],CH3NO2

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=11.7421(12)Å   b=12.8654(11)Å   c=17.8180(15)Å

α=90.00°   β=90.00°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) dinitrate mono-nitromethane solvate

C18H24FeN10,2[NO3],CH3NO2

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=11.7098(11)Å   b=12.8195(13)Å   c=17.7697(16)Å

α=90.00°   β=90.00°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) dinitrate mono-nitromethane solvate

C18H24FeN10,2[NO3],CH3NO2

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=11.6229(10)Å   b=12.6878(12)Å   c=17.5957(19)Å

α=90.00°   β=90.00°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) dinitrate mono-nitromethane solvate

C18H24FeN10,2[NO3],CH3NO2

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=11.6168(10)Å   b=12.6034(14)Å   c=17.4840(19)Å

α=90.00°   β=90.00°   γ=90.00°

(Tris-(4-(pyrazol-3-yl)-3-aza-3-butenyl)amine)iron(ii) dinitrate mono-nitromethane solvate

C18H24FeN10,2[NO3],CH3NO2

Lazar, Hanane Z.Forestier, ThibautBarrett, Simon A.Kilner, Colin A.Létard, Jean-FrançoisHalcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2007) 38 4276-4285

a=11.626(2)Å   b=12.574(2)Å   c=17.373(3)Å

α=90.00°   β=90.00°   γ=90.00°

Bis[2,6-di(pyrazol-1-yl)pyridine]iron(II) hemiiodide sesqui(triiodide)

[C22H18FeN10],I0.5,[I3]1.5

Elhaïk, JérômeKilner, Colin A.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2006) 6 823-830

a=15.9084(3)Å   b=13.6094(3)Å   c=15.1155(2)Å

α=90.00°   β=104.3473(8)°   γ=90.00°

Bis[2,6-bis(3-methylpyrazol-1-yl)pyridine]iron(II) dihexafluoroantimonate

C26H26FeN10,2[F6Sb]

Elhaïk, JérômeKilner, Colin A.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2006) 6 823-830

a=19.7007(4)Å   b=11.1095(2)Å   c=16.8557(2)Å

α=90.00°   β=110.9156(6)°   γ=90.00°

Bis[2,6-(3-methylpyrazol-1-yl)pyridine]iron(II) diperchlorate acetone solvate

C26H26FeN10,2[ClO4],C3H6O

Elhaïk, JérômeKilner, Colin A.Halcrow, Malcolm A.

Dalton transactions (Cambridge, England : 2003) (2006) 6 823-830

a=23.1702(4)Å   b=11.1910(2)Å   c=28.3275(5)Å

α=90.00°   β=107.0868(9)°   γ=90.00°